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Beilstein J. Org. Chem. 2021, 17, 2477–2487, doi:10.3762/bjoc.17.164
Graphical Abstract
Figure 1: Structures of azide and alkyne functional molecules and polymers used in the photoinduced CuAAC rea...
Figure 2: UV–vis spectra of CuICl, CuIICl2 and BPNs.
Figure 3: a) 1H NMR spectra of the model reaction between benzyl azide (Az-1) and phenylacetylene (Alk-3) bef...
Scheme 1: Proposed mechanism for photoinduced CuAAC reaction using exfoliated BPNs.
Figure 4: a) 1H NMR spectrum of chain end modified PCL-Anth; b) UV–vis spectra of (azidomethyl)anthracene (bl...
Scheme 2: Synthesis of PS-b-PCL block copolymer via exfoliated BPNs-mediated photoinduced CuAAC reaction.
Figure 5: a) GPC traces of PS-Az, PCL-Alk and block copolymer (Ps-b-PCL) b) 1H NMR spectrum of the block copo...
Scheme 3: Preparation of the cross-linked polymer by CuAAC reaction using multifunctional monomers, Az-3 and ...
Figure 6: a) DSC thermogram of photoinduced synthesis of nanocomposite networks (heating rate: 10 °C/min). b)...
Figure 7: (a, b) TEM images of cross-linked polymer at two different magnifications, c) HAADF-STEM image and ...